HRID1871923

反应详情

EQUATION

反应方程式

HRID 1871923 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

4-(2-Quinolylmethylene)piperidine (9.62 g) was dissolved in ethanol (500 ml), and 10% palladium-carbon (1.9 g) was added to the solution. The mixture was stirred under a hydrogen stream at room temperature for 90 minutes. After removal of the catalyst by filtration, the filtrate was concentrated under reduced pressure, to thereby obtain the title compound as a colorless solid.

WORKUP

后处理

  1. customAfter removal of the catalyst
  2. filtrationby filtration
  3. concentrationthe filtrate was concentrated under reduced pressure