HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18689938, compound → HCID 18689941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18689938 | HCID 18689938 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18689941 | HCID 18689941 | — |
Reaction Steps
4-(2-Quinolylmethylene)piperidine (9.62 g) was dissolved in ethanol (500 ml), and 10% palladium-carbon (1.9 g) was added to the solution. The mixture was stirred under a hydrogen stream at room temperature for 90 minutes. After removal of the catalyst by filtration, the filtrate was concentrated under reduced pressure, to thereby obtain the title compound as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107308 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-1028fdb0ad1a4cc5b26e5373dedba277 |
| Source note | uspto-grants-2000_08 |