HRID1871947

反应详情

EQUATION

反应方程式

HRID 1871947 的结构方程式

PROCEDURE

实验过程

By the procedure described in Aa) to Ac), the intermediate product 4-(2-furylmethylthio)-2-hydroxymethyl-3-methoxypyridine is obtained starting from 4-chloro-3-methoxy-2-methylpyridine N-oxide; m.p. 56-58° C. Chlorination with thionyl chloride by the procedure described in Example Ad) gives the title compound as a beige powder; m.p. 135° C. (decomp.).

WORKUP

后处理

  1. customis obtained