HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57299275, compound → HCID 18689715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57299275 | HCID 57299275 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 18689715 | HCID 18689715 | — |
Reaction Steps
A solution of the product from example 28 step (ii) (0.07 g) in dichloromethane (1 ml) and trifluoroacetic acid (1 ml) was stirred overnight and evaporated. The residue was triturated with ether and filtered off. Yield 0.05 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107297 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-8a01ac1f87fd4999806f26c5380aeb5c |
| Source note | uspto-grants-2000_08 |