HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 10782556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 10641825 | HCID 10641825 | — |
| Product | HCID 10782556 | HCID 10782556 | — |
Reaction Steps
Material from Example 72 was treated with 65% sulfuric acid as described in Example 65 to give the desired product as a viscous oil. TLC on silica gel with 70:30 hexane-ethyl acetate showed Rf=0.57. Mass spec. (m+H)+ =329.0641; calcd., 329.0653 (79Br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107301 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-aa2aa14dc12c41f0863d45917981959b |
| Source note | uspto-grants-2000_08 |