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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1872246Generated: October 31, 2026

3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-azepane-2-carboxylic acid → 3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid

https://huagongshe.com/reaction/1872246

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-azepane-2-carboxylic acidHCID 18689641—
Reactant3-Hydroxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid tert butyl esterHCID 53896843—
Product3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acidHCID 18689658—

Reaction Steps

3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid was synthesized from 3-Hydroxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid tert butyl ester in the same manner as the procedures used for the preparation of 3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-azepane-2-carboxylic acid: MS (M-H)- =382.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06107291
Source datasetuspto-grants-2000_08
ORD IDord-136873d6ec9e4bc1b908d2dd452a7c35
Source noteuspto-grants-2000_08