HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxymethyl-1-(4-methoxybenzenesulfonyl)-azepane-2-carboxylic acid → 3-Hydroxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid hydroxyamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxymethyl-1-(4-methoxybenzenesulfonyl)-azepane-2-carboxylic acid | HCID 18689633 | — |
| Reactant | Acetic acid 2-hydroxycarbamoyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepin-3-ylmethyl ester | HCID 53873648 | — |
| Product | 3-Hydroxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid hydroxyamide | HCID 9841630 | — |
Reaction Steps
3-Hydroxymethyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid hydroxyamide was synthesized from Acetic acid 2-hydroxycarbamoyl-1-(4-methoxy-benzenesulfonyl)-2,3,4,7-tetrahydro-1H-azepin-3-ylmethyl ester in the same manner as the procedures used for the preparation of 3-Hydroxymethyl-1-(4-methoxybenzenesulfonyl)-azepane-2-carboxylic acid hydroxamide: MS (M-H)- =355.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107291 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-f698e69c0213446eb66835d5fc301b54 |
| Source note | uspto-grants-2000_08 |