HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → HCID 136333678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | HCID 136333680 | HCID 136333680 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 136333678 | HCID 136333678 | — |
Reaction Steps
To a mixture of 1 g of zinc 5-(4-hydroxyphenyl)-10,15,20-triphenylporphyrin and chloroform, there was added 60 μl of chlorosulfonic acid dissolved in 10 ml of chloroform at 0° C. After 12 h, the solution was poured on ice, and the organic phase was separated. Evaporation of the solvent yielded the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107480 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-b7aed0de72c345e39237fb33318f83ed |
| Source note | uspto-grants-2000_08 |