HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 11426171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 5-Aminoisoquinoline | HCID 70766 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 11426171 | HCID 11426171 | — |
Reaction Steps
To a solution of 5-aminoisoquinoline (14.4 g, 100 mmol) in acetone (300 ml) was added iodomethane (14.4 ml). The solution was briefly stirred and then allowed to sthand for 2h. The yellow precipithate was then filtered, washed with acetone and dried to afford the title compound as a yellow solid (18.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06110934 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-1393fedd38a24ce8839b7aed18fa7a4a |
| Source note | uspto-grants-2000_08 |