HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethoxybenzoyl chloride → HCID 18687443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethoxybenzoyl chloride | HCID 2734719 | — |
| Reactant | 2-Methyl-1,2,3,4-tetrahydroisoquinolin-5-amine | HCID 14171269 | — |
| Product | HCID 18687443 | HCID 18687443 | — |
Reaction Steps
To a solution of 5-amino-2-methyl-1,2,3,4-tetrahydroisoquinoline (0.25 g, 1.54 mmol) in ethyl acethate (5 ml) was added 2,4-dimethoxybenzoyl chloride (0.263 g 1.54 mmol). The mixture was stirred under argon for 2 h before the precipithate was filtered off and dried to afford the title compound as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06110934 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-c0251fcf0e494f32bc10afc48f0801c0 |
| Source note | uspto-grants-2000_08 |