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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1872710Generated: November 3, 2026

2,4-Dimethoxybenzoyl chloride → HCID 18687443, compound

https://huagongshe.com/reaction/1872710

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,4-Dimethoxybenzoyl chlorideHCID 2734719—
Reactant2-Methyl-1,2,3,4-tetrahydroisoquinolin-5-amineHCID 14171269—
ProductHCID 18687443HCID 18687443—

Reaction Steps

To a solution of 5-amino-2-methyl-1,2,3,4-tetrahydroisoquinoline (0.25 g, 1.54 mmol) in ethyl acethate (5 ml) was added 2,4-dimethoxybenzoyl chloride (0.263 g 1.54 mmol). The mixture was stirred under argon for 2 h before the precipithate was filtered off and dried to afford the title compound as white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06110934
Source datasetuspto-grants-2000_08
ORD IDord-c0251fcf0e494f32bc10afc48f0801c0
Source noteuspto-grants-2000_08