HRID1872783

反应详情

EQUATION

反应方程式

HRID 1872783 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 3-ethyl-2-nitro-4-trifluoroacetamidophenol (18.21 mmol) and 10% palladium-on-carbon (0.45 g) in methanol (100 mL) is shaken under an atmosphere of hydrogen (50 psi) for three hours. The mixture is filtered through Celite and concentrated under reduced pressure to yield 2-amino-3-ethyl. trifluoroacetamidophenol.

WORKUP

后处理

  1. filtrationThe mixture is filtered through Celite
  2. concentrationconcentrated under reduced pressure
  3. customto yield 2-amino-3-ethyl