HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54107403, compound → HCID 53868867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54107403 | HCID 54107403 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 53868867 | HCID 53868867 | 68.3% |
Reaction Steps
A mixture of (S)-3-azidohexadecanamide (0.17 g) and 10% palladium on carbon (20 mg) was hydrogenated at atmospheric pressure for 5 hours. The catalyst was filtered off with celite, and the filtrate was concentrated under reduced pressure. The residue was recrystallized from ethyl acetate (3 ml) to give (S)-3-aminohexadecanamide (106 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06110933 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-1396332d6bd8465fb69820c96fe977fc |
| Source note | uspto-grants-2000_08 |