Water → 2-Hydroxypentadecanamide

HRID 1872804Notes

Reaction equation

HRID 1872804 reaction equation
[OH:1][CH:2]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[C:3]#[N:4].[OH2:18]>Cl>[OH:1][CH:2]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[C:3]([NH2:4])=[O:18]

Participants

4

Reactant 2

HCID 962WaterHCID 18687295HCID 18687295, compound

Product 1

HCID 186871972-Hydroxypentadecanamide

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

2-Hydroxypentadecanenitrile (1.0 g) was suspended in concentrated hydrochloric acid (15 ml), and this suspension was vigorously stirred at room temperature for 24 hours. Then, this mixture was diluted with water (45 ml). The insoluble powder was collected by filtration, washed with water (10 ml×3), and dried to give 2-hydroxypentadecanamide (1.06 g).

Workup

  1. filtrationThe insoluble powder was collected by filtration
  2. washwashed with water (10 ml×3)
  3. customdried

Sources & evidence

ORD record
ord-34368b5e0f834ae0af1d4779e4c457cb
Source dataset
uspto-grants-2000_08
Patent number
US06110933

Reaction notes

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