Methyl bromoacetate → HCID 9826477, compound

HRID 1872861Notes

Reaction equation

[Br:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([C:12]([C:14]3[C:18]4[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=4[O:16][C:15]=3[CH2:23][CH2:24][CH2:25][CH3:26])=[O:13])=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[OH:27].Br[CH2:29][C:30]([O:32]C)=[O:31]>>[Br:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([C:12]([C:14]3[C:18]4[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=4[O:16][C:15]=3[CH2:23][CH2:24][CH2:25][CH3:26])=[O:13])=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[O:27][CH2:29][C:30]([OH:32])=[O:31]

Participants

Reactant 2

HCID 60984Methyl bromoacetate

HCID 10526273HCID 10526273, compound

Product 1

HCID 9826477HCID 9826477, compound

Procedure

The title compound was prepared from 1-bromo-6-(2-butyl-benzofuran-3-carbonyl)-naphthalen-2-ol, and methyl bromoacetate, in substantially the same manner, as described in Example 4, and was obtained as a white solid, mp 163-165° C.; MS m/e 680 (M+);

Workup

customwas obtained as a white solid, mp 163-165° C.

Sources & evidence

ORD record: ord-bdeb298f64b14919864fc31e19e36c4a
Source dataset: uspto-grants-2000_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06110963

Reaction notes

Loading…