Methyl bromoacetate → HCID 9867355, compound

HRID 1872864Notes

Reaction equation

[CH2:1]([C:5]1[O:6][C:7]2[CH:28]=[CH:27][CH:26]=[CH:25][C:8]=2[C:9]=1[CH:10]([OH:24])[C:11]1[CH:16]=[CH:15][C:14]([C:17]2[CH:22]=[CH:21][C:20]([OH:23])=[CH:19][CH:18]=2)=[CH:13][CH:12]=1)[CH2:2][CH2:3][CH3:4].Br[CH2:30][C:31]([O:33]C)=[O:32]>>[CH2:1]([C:5]1[O:6][C:7]2[CH:28]=[CH:27][CH:26]=[CH:25][C:8]=2[C:9]=1[CH:10]([OH:24])[C:11]1[CH:16]=[CH:15][C:14]([C:17]2[CH:22]=[CH:21][C:20]([O:23][CH2:30][C:31]([OH:33])=[O:32])=[CH:19][CH:18]=2)=[CH:13][CH:12]=1)[CH2:2][CH2:3][CH3:4]

Participants

Reactant 2

HCID 60984Methyl bromoacetate

HCID 9842446HCID 9842446, compound

Product 1

HCID 9867355HCID 9867355, compound

Procedure

The title compound was prepared from 4'-[(2-butyl-benzofuran-3-yl)-hydroxymethyl]-biphenyl-4-ol, and methyl bromoacetate in substantially the same manner, as described in Example 4, and was obtained as a yellow solid, mp 111-113° C.; MS m/e 430 (M+);

Workup

customwas obtained as a yellow solid, mp 111-113° C.

Sources & evidence

ORD record: ord-3116a794cac248718a1d5bc7a6482cf5
Source dataset: uspto-grants-2000_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06110963

Reaction notes

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