HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58151927, compound → HCID 58151932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58151927 | HCID 58151927 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58151932 | HCID 58151932 | — |
Reaction Steps
76.0 g (0.26 mol) of 5,6-difluoro-3-(4-propylcyclohexyl)-1,2-dihydronaphthalene are hydrogenated at RT and atmospheric pressure for 19 h in 500 ml of THF in the presence of Pd/C (5% of Pd). The reaction solution is filtered and evaporated to dryness. The residue is used for the following reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08303844B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-560499e664ea49bb9a9f51cff2d506e8 |
| Source note | uspto-grants-2012_11 |