HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminopyridine → HCID 59161030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminopyridine | HCID 1727 | — |
| Reactant | (6-Bromopyridin-2-yl)methanol | HCID 3517811 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 59161030 | HCID 59161030 | — |
Reaction Steps
1.35 g (14.3 mmol) of 4-aminopyridine and 1.34 g (7.1 mmol) of (6-bromopyridin-2-yl)methanol are stirred at 150° C. for 4 h. After cooling to RT, 50 ml of acetonitrile are added and the reaction mixture is stirred for 20 min. The precipitate formed is filtered off with suction at 0° C. and washed with 10 ml of acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08304412B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-b5c6e61fd8914dd09e88ce08d61b33b8 |
| Source note | uspto-grants-2012_11 |