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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1873578Generated: November 2, 2026

4-Aminopyridine → HCID 59161030, compound

https://huagongshe.com/reaction/1873578

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-AminopyridineHCID 1727—
Reactant(6-Bromopyridin-2-yl)methanolHCID 3517811—
SolventAcetonitrileHCID 6342—
ProductHCID 59161030HCID 59161030—

Reaction Steps

1.35 g (14.3 mmol) of 4-aminopyridine and 1.34 g (7.1 mmol) of (6-bromopyridin-2-yl)methanol are stirred at 150° C. for 4 h. After cooling to RT, 50 ml of acetonitrile are added and the reaction mixture is stirred for 20 min. The precipitate formed is filtered off with suction at 0° C. and washed with 10 ml of acetonitrile.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08304412B2
Source datasetuspto-grants-2012_11
ORD IDord-b5c6e61fd8914dd09e88ce08d61b33b8
Source noteuspto-grants-2012_11