Thionyl Chloride → HCID 59160958, compound

Participants

Reaction Steps

50 mg (0.22 mmol) of the compound from Example 35A and 53 mg (0.44 mmol) of thionyl chloride are initially charged at 0° C. in 1.5 ml of dichloromethane and, after warming to RT, stirred at this temperature for 12 h. The solvent is removed on a rotary evaporator and the product that remains is directly reacted further.

Provenance & Evidence