HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 24961262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 3-Chloromethyl-benzamide | HCID 737145 | — |
| Reactant | HCID 24959059 | HCID 24959059 | — |
| Reactant | HCID 178510477 | HCID 178510477 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 24961262 | HCID 24961262 | — |
Reaction Steps
50 mg (0.14 mmol) of the compound from Example 31A, 36 mg (0.21 mmol) of 3-(chloromethyl)benzamide and 48 mg (0.58 mmol) of sodium bicarbonate in 2.0 ml of dry DMF are reacted analogously to the preparation of the compound of Example 14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08304412B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-cb6cbfdecfad4ef4b593703e6f2fe26b |
| Source note | uspto-grants-2012_11 |