HRID1873687
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
CONDITIONS
反应条件
- 温度
- 70 °C
PROCEDURE
实验过程
Compound 1d (88.0 mg) was dissolved in 4N HCl-dioxane solution, followed by stirring at 70° C. for 1 hour. The precipitate in the reaction mixture was filtrated, to thereby yield compound 1e (67.1 mg, yield: 79%).
WORKUP
后处理
- filtrationThe precipitate in the reaction mixture was filtrated