3-Isopropoxypropylamine → HCID 86650701, compound

Participants

Reaction Steps

Compound 1e (13.2 mg), 3-isopropoxypropylamine (9.11 μL), and 4-(5,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholine hydrochloride n-hydrate (hereinafter referred to as DMTMM•n-hydrate) (8.67 mg) were dissolved in tetrahydrofuran (1 mL), followed by stirring at room temperature for 2 hours. The reaction mixture was distilled under reduced pressure, and water was added to the residue. The precipitate was filtrated, to thereby yield the titled compound 1 (11.6 mg, yield: 79%).

Provenance & Evidence