HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbazate → HCID 67159661, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Reactant | 2-Cyclopropyl-2-hydroxyacetonitrile | HCID 11389359 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67159661 | HCID 67159661 | — |
Reaction Steps
Cyclopropylcarboxaldehyde (4.07 mL, 14.3 mmol) is dissolved in 3 mL MeOH and tert-butylcarbazate (1.89 g, 14.3 mmol) is added. The reaction mixture is stirred overnight at RT and subsequently concentrated in vacuo. Yield: 2.57 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08304556B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-91b69c770b414e77b1c0bda271a27ff0 |
| Source note | uspto-grants-2012_11 |