Ethyl ketone → HCID 11788888, compound

HRID 1874083Notes

Reaction equation

HRID 1874083 reaction equation
[CH3:1][CH2:2][C:3](=O)[CH2:4][CH3:5].[C:7]([O:11][C:12](=[O:15])[NH:13][NH2:14])([CH3:10])([CH3:9])[CH3:8]>>[C:7]([O:11][C:12]([NH:13][N:14]=[C:3]([CH2:4][CH3:5])[CH2:2][CH3:1])=[O:15])([CH3:10])([CH3:9])[CH3:8]

Participants

3

Reactant 2

HCID 7288Ethyl ketoneHCID 70091tert-Butyl carbazate

Product 1

HCID 11788888HCID 11788888, compound

Procedure

B-20a is prepared analogously to B-19a starting from 3-pentanone (1.23 mL, 11.6 mmol) and tert-butylcarbazate (1.53 g, 11.6 mmol). Yield: 2.26 g.

Workup

  1. customB-20a is prepared analogously to B-19a

Sources & evidence

ORD record
ord-e6c618f3108143658e4a9e1264787685
Source dataset
uspto-grants-2012_11
Patent number
US08304556B2

Reaction notes

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