HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbazate → HCID 67160005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Reactant | 1-Cyclopropylpiperidin-4-one | HCID 16227629 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67160005 | HCID 67160005 | — |
Reaction Steps
A mixture of 1-cyclopropyl-4-piperidon (10.0 g. 71.8 mmol) and tert-butylcarbazate (9.50 g, 71.8 mmol) in 25 mL THF is stirred for 3 h at RT and then concentrated in vacuo. Yield: 19.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08304556B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-a9f6746ddbda4150adca5fb2dd560b26 |
| Source note | uspto-grants-2012_11 |