HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanatoformate → Ethyl {[(5-methoxypyridin-2-yl)amino]carbonothioyl}carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanatoformate | HCID 85320 | — |
| Reactant | 2-Amino-5-methoxypyridine | HCID 11320934 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | Ethyl {[(5-methoxypyridin-2-yl)amino]carbonothioyl}carbamate | HCID 58087980 | 62.3% |
Reaction Steps
In the same manner as in Reference Example 30 and using 5-methoxypyridin-2-amine (1.05 g, 8.43 mmol), DMSO (5 mL) and ethyl isothiocyanatoformate (1.44 g, 11.0 mmol) as starting materials, the title compound (1.34 g, 62%) was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08304557B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-d17d96f9c49d44fb8712564c06747c51 |
| Source note | uspto-grants-2012_11 |