6-Chloro-2-fluoro-3-methylphenol → HCID 86644936, compound

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The title compound was prepared in a similar manner to that described herein using 6-chloro-2-fluoro-3-methylphenol (0.60 g, 3.74 mmol) and 6-chloro-4-nitro-2-pyridinecarbonitrile (0.69 g, 3.74 mmol) to give the title compound as a white solid (0.98 g, 88%). 1H NMR (400 MHz, CHLOROFORM-d) δ ppm 7.20-7.24 (1H, m) 7.16 (1H, d) 7.14 (1H, d) 6.98 (1H, d) 2.33 (3H, d). LCMS: m/z 297 (M+1).

Provenance & Evidence