HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 68590834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Thieno[2,3-c]pyridine, 4,5-dihydro-7-methyl- (5CI) | HCID 57423976 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68590834 | HCID 68590834 | — |
Reaction Steps
A mixture of 4.64 g (31 mmol) 7-methyl-4,5-dihydro-thieno[2,3-c]pyridine (prepared analogously to J.Am.Chem.Soc., 1951, 1257), 8.0 ml (128 mmol) methyl iodide and 20 ml of ethyl acetate is stirred for 15 min. The precipitate formed is suction filtered, washed with ethyl acetate and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309542B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-0843bf2fcfc94ff0ada02d33864cdc05 |
| Source note | uspto-grants-2012_11 |