HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59279969, compound → HCID 59279901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59279969 | HCID 59279969 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59279901 | HCID 59279901 | — |
Reaction Steps
0% Pd/C (4 mg, 0.004 mmol) was added to a solution of the product from Step 1 (25 mg, 0.038 mmol) in EtOH (3 mL), and the mixture was placed under H2. After 18 hours, the mixture was filtered through a pad of glass wool, and the solvent was removed in vacuo. LRMS ESI+ (M+H)+ 654.5; calcd for C36H52N3O8: 654.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309540B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-e1253c9622e348f597fdfa4955918341 |
| Source note | uspto-grants-2012_11 |