Hydrochloric Acid → HCID 68665125, compound

Participants

Reaction Steps

A solution of the product from Step 5 (25.2 g, 31.6 mmol) in 4.0 N HCl in dioxane (400 mL) was stirred for 6 hours. N2 was bubbled through the solution for 15 minutes, and the solvent was concentrated in vacuo to give 20.3 g of the title compound as a thick oil. LRMS ESI+ (M+H−2(HCl))+ 642.3, calcd for C34H48N3O9: 642.3.

Provenance & Evidence