Thionyl Chloride → HCID 23144827, compound

HRID 1875554Notes

Reaction equation

HRID 1875554 reaction equation
Cl.[CH3:2][N:3]([CH2:5][C:6]1[C:7]([N+:15]([O-:17])=[O:16])=[C:8]([CH:12]=[CH:13][CH:14]=1)[C:9](O)=[O:10])[CH3:4].S(Cl)([Cl:20])=O>>[CH3:2][N:3]([CH2:5][C:6]1[C:7]([N+:15]([O-:17])=[O:16])=[C:8]([CH:12]=[CH:13][CH:14]=1)[C:9]([Cl:20])=[O:10])[CH3:4]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 69203826HCID 69203826, compound

Product 1

HCID 23144827HCID 23144827, compound

Conditions

Temperature
80 °C

Procedure

The mixture of 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride (0.1 g) and thionylchloride (5 mL) was stirred at 80° C. for 3 hours. The solvent was removed and the residue was dried to obtain 3-dimethylamino methyl-2-nitrobenzoyl chloride.

Workup

  1. customThe solvent was removed
  2. customthe residue was dried

Sources & evidence

ORD record
ord-dbbba8b3f9234078905a6bdb7e95cc15
Source dataset
uspto-grants-2012_11
Patent number
US08309561B2

Reaction notes

Loading…