Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 69203826 | HCID 69203826 | — |
| Product | HCID 23144827 | HCID 23144827 | — |
Reaction Steps
The mixture of 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride (0.1 g) and thionylchloride (5 mL) was stirred at 80° C. for 3 hours. The solvent was removed and the residue was dried to obtain 3-dimethylamino methyl-2-nitrobenzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08309561B2 |
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| Source dataset | uspto-grants-2012_11 |
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| ORD ID | ord-dbbba8b3f9234078905a6bdb7e95cc15 |
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| Source note | uspto-grants-2012_11 |
|---|