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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1875554Generated: October 30, 2026

Thionyl Chloride → HCID 23144827, compound

https://huagongshe.com/reaction/1875554

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 69203826HCID 69203826—
ProductHCID 23144827HCID 23144827—

Reaction Conditions

Temperature80 °C

Reaction Steps

The mixture of 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride (0.1 g) and thionylchloride (5 mL) was stirred at 80° C. for 3 hours. The solvent was removed and the residue was dried to obtain 3-dimethylamino methyl-2-nitrobenzoyl chloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08309561B2
Source datasetuspto-grants-2012_11
ORD IDord-dbbba8b3f9234078905a6bdb7e95cc15
Source noteuspto-grants-2012_11