HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-4-methoxybenzene → 1-Cyclohexylmethyl-2-[2-(4-methoxy-phenylethynyl)-phenyl]-1H-benzoimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-4-methoxybenzene | HCID 251020 | — |
| Reactant | HCID 67050067 | HCID 67050067 | — |
| Product | 1-Cyclohexylmethyl-2-[2-(4-methoxy-phenylethynyl)-phenyl]-1H-benzoimidazole | HCID 67050148 | — |
Reaction Steps
The title compound was prepared in analogy to Example 72, intermediate a, from 2-(2-bromo-phenyl)-1-cyclohexylmethyl-1H-benzoimidazole and 1-ethynyl-4-methoxy-benzene (CAS Reg. No. 768-60-5). Yellow sticky solid (24%). MS (Turbo Spray): m/z=421.4 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309581B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-947fd255b8804d8084ac59a53f04b3f0 |
| Source note | uspto-grants-2012_11 |