HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → HCID 3866276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | 2,4-Dichloroquinazoline | HCID 252886 | — |
| Product | HCID 3866276 | HCID 3866276 | — |
Reaction Steps
The title compound was prepared from 2,4-dichloroquinazoline (50 mg, 0.251 mmol) and 4-methoxyaniline (45 mg, 0.326 mmol) by a procedure similar to Example 1b and was isolated as off white powder (55 mg, 77%). 1H NMR (CDCl3): 10.25 (s, 1H), 8.58 (d, J=8.4 Hz, 1H), 7.88 (t, J=7.2 Hz, 1H), 7.71-7.63 (m, 4H), 7.03-6.99 (m, 2H), 3.79 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309562B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-21088177793c4da4a5f206d28336a3d6 |
| Source note | uspto-grants-2012_11 |