HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methyl-4-anisidine → HCID 178492251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methyl-4-anisidine | HCID 22250 | — |
| Reactant | 6-chloro-1H-purin-2-amine | HCID 178508435 | — |
| Product | HCID 178492251 | HCID 178492251 | — |
Reaction Steps
The title compound was prepared from 2-amino-6-chloro-9H-purine (100 mg, 0.546 mmol) and 4-methoxy-N-methyl-aniline (127 mg, 0.656 mmol) by a procedure similar to Example 1b and was isolated as white powder (5 mg, 5%). 1H NMR (CDCl3): 7.54 (s, 1H), 7.25 (d, J=8.7 Hz, 2H), 6.98 (d, J=8.7 Hz, 2H), 3.86 (s, 3H), 3.66 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309562B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-54921ed317624af3a0bd68a459052d80 |
| Source note | uspto-grants-2012_11 |