Acetic Acid → HCID 68478950, compound

Participants

Reaction Steps

A solution of 1-(2-Cyclohexyl-ethyl)-isatine (170 mg, 0.73 mmol) previously obtained (see isatine 3 in table 5) and Benzenesulfonyl hydrazide (126 mg, 0.73 mmol) in 19 ml of a solution of acetic acid, ethanol and THF (20%, 40%, 40%) is stirred at room temperature for 12 h. After concentration, a yellow precipitate is filtered and washed with ethanol to afford a desired product. M: 54 mg, Yield: 20%

Provenance & Evidence