Benzoylhydrazine → HCID 178487276, compound

HRID 1876263Notes

Reaction equation

HRID 1876263 reaction equation
[CH2:1]([N:8]1[C:18]2[C:13](=[CH:14][CH:15]=[C:16]([O:19][CH3:20])[CH:17]=2)[C:11](=O)[C:9]1=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:21]([NH:29][NH2:30])(=[O:28])[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[CH2:1]([N:8]1[C:18]2[C:13](=[CH:14][CH:15]=[C:16]([O:19][CH3:20])[CH:17]=2)/[C:11](=[N:30]/[NH:29][C:21](=[O:28])[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)/[C:9]1=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 11955BenzoylhydrazineHCID 61356413HCID 61356413, compound

Product 1

HCID 178487276HCID 178487276, compound

Procedure

The title compound was prepared as a yellow solid, using 1- benzyl-6-methoxy-isatin and benzhydrazide according to the synthetic method E. 1H NMR (CDCl3): δ 3.77 (s, 3H), 4.94 (s, 2H), 6.35 9d, 1H), 6.62 (dd, 1H), 7.29-7.36 (m, 4H), 7.51 (t, 2H), 7.59 (t, 1H), 7.80 (d, 1H), 8.01 (d, 2H), 13.95 (br s, 1H).

Sources & evidence

ORD record
ord-9cf8e6f53ee94cd6bac2504f84efe1f7
Source dataset
uspto-grants-2012_11
Patent number
US08309595B2

Reaction notes

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