Benzoylhydrazine → HCID 178448702, compound

HRID 1876265Notes

Reaction equation

[CH2:1]([N:5]1[C:15]2[C:10](=[CH:11][CH:12]=[C:13]([O:16][CH3:17])[CH:14]=2)[C:8](=O)[C:6]1=[O:7])[CH2:2][CH2:3][CH3:4].[C:18]([NH:26][NH2:27])(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH2:1]([N:5]1[C:15]2[C:10](=[CH:11][CH:12]=[C:13]([O:16][CH3:17])[CH:14]=2)/[C:8](=[N:27]/[NH:26][C:18](=[O:25])[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)/[C:6]1=[O:7])[CH2:2][CH2:3][CH3:4]

Participants

Reactant 2

HCID 11955Benzoylhydrazine

HCID 25194457HCID 25194457, compound

Product 1

HCID 178448702HCID 178448702, compound

Procedure

The title compound was prepared as a yellow solid, using 1- butyl-6-methoxy-isatin and benzhydrazide according to the synthetic method E. NMR (CDCl3): δ 0.98 (t, 3H), 1.38 to 1.45 (m, 4H), 1.67-1.73 (m, 2H), 3.73 (t, 2H), 3.87 (s, 3H), 6.44 (d, 1H), 6.64 (dd, 1H), 7.51 (t, 2H), 7.59 (t, 1H), 7.80 (d, 1H), 8.00 (d, 1H), 13.97 (br s, 1H).

Sources & evidence

ORD record: ord-edb9848ecf6b44be8590d4eac75b8626
Source dataset: uspto-grants-2012_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08309595B2

Reaction notes

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