Benzoylhydrazine → HCID 178487282, compound

HRID 1876267Notes

Reaction equation

[CH:1]1([CH2:7][CH2:8][N:9]2[C:19]3[C:14](=[CH:15][CH:16]=[C:17]([O:20][CH3:21])[CH:18]=3)[C:12](=O)[C:10]2=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:22]([NH:30][NH2:31])(=[O:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[CH:1]1([CH2:7][CH2:8][N:9]2[C:19]3[C:14](=[CH:15][CH:16]=[C:17]([O:20][CH3:21])[CH:18]=3)/[C:12](=[N:31]/[NH:30][C:22](=[O:29])[C:23]3[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=3)/[C:10]2=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

Reactant 2

HCID 11955Benzoylhydrazine

HCID 25194458HCID 25194458, compound

Product 1

HCID 178487282HCID 178487282, compound

Procedure

The title compound was prepared as a yellow solid, using 1-(2-cyclohexylethyl)-6-methoxy-isatin and benzhydrazide according to the synthetic method E. NMR (CDCl3): δ 0.96-1.04 (m, 2H), 1.15-1.38 (m, 4H), 1.59 (dd, 2H), 1.65-1.75 (m,3H), 1.81 (d, 2H), 3.74 (t, 2H), 3.87 (s, 3H), 6.43 (d, 1H), 6.64 (dd, 1H), 7.51 (t, 2H), 7.59 (t, 1H), 7.80 (d, 1H), 8.00 (d, 1H), 13.96 (br s, 1H).

Sources & evidence

ORD record: ord-a8ac9cd5b7724b7bb81f8343b7bde331
Source dataset: uspto-grants-2012_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08309595B2

Reaction notes

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