HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Cyclohexylacetohydrazide → HCID 178446194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Cyclohexylacetohydrazide | HCID 3818673 | — |
| Reactant | 1-Pentyl-6-methoxy-isatin | HCID 25194456 | — |
| Product | HCID 178446194 | HCID 178446194 | — |
Reaction Steps
The title compound was prepared as a yellow solid, using 1-pentyl-6-methoxy-isatin obtained in Example 39(A) and 2-cyclohexylacetohydrazide according to the synthetic method E. NMR (CDCl3): δ 0.91 (t, 3H), 1.01-1.07 (m, 2H), 1.18 to 1.39 (m, 7H), 1.60-1.72 (m, 5H), 1.81 (d, 2 H), 1.92-1.94 (m, 1H), 2.27 (d, 1H), 2.69 (d, 1H), 3.70 (t, 2H), 3.87 (s, 3H), 6.42 (s, 1H), 6.62 (d, 1H), 7.52 and 7.74 (d for isomers, 1H), 12.39 and 13.99 (br s for isomers, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309595B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-2c34ba923b904edeaea85f2f14a0aa7e |
| Source note | uspto-grants-2012_11 |