Hydroxylamine → Cyclododecanone, oxime

HRID 1876764Notes

Reaction equation

[C:1]1(=O)[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[NH2:14][OH:15]>>[C:1]1(=[N:14][OH:15])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

Reactant 2

HCID 787Hydroxylamine

HCID 13246Cyclododecanone

Product 1

HCID 136762Cyclododecanone, oxime

Procedure

reacting cyclododecanone with hydroxylamine in an aqueous solution in the presence of an organic solvent (hereinafter, referred to as “oxime-formation solvent”) to produce cyclododecanone oxime (hereinafter, referred to as an “oxime-forming step”);

Sources & evidence

ORD record: ord-09019b12847d4637a771d34616606c20
Source dataset: uspto-grants-2012_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08309714B2

Reaction notes

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