HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → HCID 86655425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | 3-[(6-Chloro-3-pyridinyl)methyl]-2-thiazolidinimine | HCID 9859386 | — |
| Product | HCID 86655425 | HCID 86655425 | — |
Reaction Steps
A mixture of 3-(2-Chloro-5-pyridinylmethyl)-2-iminothiazolidine (227 mg, 1.1 mmol) and 10 ml of ethyl formate was heated at the boiling point of ethyl formate for 5 hours with stirring. After distilling the excessive ethyl formate off followed by purification by a silica gel column chromatography, the resultant intended solid was washed with diethyl ether. Yield: 32 mg (13%). Melting point: 99-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309733B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-db1f94d3905947dbbed3f1d7bfda6a1f |
| Source note | uspto-grants-2012_11 |