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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1877022Generated: November 2, 2026

Thionyl Chloride → HCID 68514193, compound

https://huagongshe.com/reaction/1877022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 68507584HCID 68507584—
SolventTolueneHCID 1140—
ProductHCID 68514193HCID 68514193100%

Reaction Steps

To a solution of cyclohexyl[2-methyl-5-(pyridin-3-yl)furan-3-yl]methanol (1.6 g) in toluene (20 mL) was added thionyl chloride (1.3 mL), and the mixture was stirred at room temperature for 4 hr. The solvent was evaporated under reduced pressure to give the title compound (1.7 g, 100%) as an amorphous compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08309580B2
Source datasetuspto-grants-2012_11
ORD IDord-c1fbc15b29ca4dccbdefcb85694993da
Source noteuspto-grants-2012_11