HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 68514191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 68515304 | HCID 68515304 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68514191 | HCID 68514191 | 100% |
Reaction Steps
To a solution of cyclohexyl[2-methyl-5-(pyridin-4-yl)furan-3-yl]methanol (0.9 g) in toluene (10 mL) was added thionyl chloride (0.7 mL), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (0.9 g, 100%) as a yellow crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-88a8b347b9b2474394e9b53b1e517b31 |
| Source note | uspto-grants-2012_11 |