HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 68511060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 68509119 | HCID 68509119 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68511060 | HCID 68511060 | 100% |
Reaction Steps
To a solution of cyclohexyl[2-methyl-5-(pyridin-2-yl)furan-3-yl]methanol (0.7 g) in toluene (20 mL) was added thionyl chloride (1.3 mL), and the mixture was stirred at room temperature for 2 hr. The solvent was evaporated under reduced pressure to give the title compound (0.8 g, 100%) as a yellow crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-3636d3b4206448ab837005979a778d5e |
| Source note | uspto-grants-2012_11 |