HRID1877059

反应详情

EQUATION

反应方程式

HRID 1877059 的结构方程式

CONDITIONS

反应条件

温度
0 °C

PROCEDURE

实验过程

To a solution of 3-amino-2-hydroxypropanoic acid (0.7 g) in methanol (15 mL) was added thionyl chloride (2.5 mL) at 0° C., and the mixture was stirred at 0° C. for 2 hr and then at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (1.6 g, 100%) as an oil.

WORKUP

后处理

  1. customat room temperature
  2. customovernight
  3. customThe solvent was evaporated under reduced pressure