HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 68509793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 68511337 | HCID 68511337 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68509793 | HCID 68509793 | 100% |
Reaction Steps
To a solution of cyclohexyl{3-methyl-5-[4-(trifluoromethyl)phenyl]thiophen-2-yl}methanol (1.3 g) in toluene (20 mL) was added thionyl chloride (0.4 mL), and the mixture was stirred at room temperature for 2 hr. The solvent was evaporated under reduced pressure to give the title compound (1.3 g, 100%) as an amorphous compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-6b78e72c6aad44bf97ba83b97b131f1a |
| Source note | uspto-grants-2012_11 |