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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1877229Generated: October 31, 2026

Thionyl Chloride → HCID 68509793, compound

https://huagongshe.com/reaction/1877229

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 68511337HCID 68511337—
SolventTolueneHCID 1140—
ProductHCID 68509793HCID 68509793100%

Reaction Steps

To a solution of cyclohexyl{3-methyl-5-[4-(trifluoromethyl)phenyl]thiophen-2-yl}methanol (1.3 g) in toluene (20 mL) was added thionyl chloride (0.4 mL), and the mixture was stirred at room temperature for 2 hr. The solvent was evaporated under reduced pressure to give the title compound (1.3 g, 100%) as an amorphous compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08309580B2
Source datasetuspto-grants-2012_11
ORD IDord-6b78e72c6aad44bf97ba83b97b131f1a
Source noteuspto-grants-2012_11