HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 68515580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 68515326 | HCID 68515326 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68515580 | HCID 68515580 | 100% |
Reaction Steps
To a solution of cyclohexyl(3-methyl-5-phenylthiophen-2-yl)methanol (0.8 g) in toluene (20 mL) was added thionyl chloride (0.3 mL), and the mixture was stirred at room temperature for 2 hr. The solvent was evaporated under reduced pressure to give the title compound (0.9 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-f85d98e9a7ef4c7097e034117e0050aa |
| Source note | uspto-grants-2012_11 |