HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58239605, compound → HCID 58239595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58239605 | HCID 58239605 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58239595 | HCID 58239595 | — |
Reaction Steps
4-[4′-Benzyloxy-5-(4-hydroxybut-1-ynyl)biphenyl-3-yl]but-3-yn-1-ol is dissolved in THF and hydrogenated to completion on a palladium/activated carbon catalyst. The catalyst is filtered off, the filtrate is evaporated in vacuo, and the residue is filtered through silica gel with toluene/ethyl acetate (1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08313669B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-00c31e0958ed40879b547a284e790ca1 |
| Source note | uspto-grants-2012_11 |