HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chlorophenylhydrazine hydrochloride → HCID 58277354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chlorophenylhydrazine hydrochloride | HCID 75331 | — |
| Reactant | HCID 58277340 | HCID 58277340 | — |
| Product | HCID 58277354 | HCID 58277354 | 33% |
Reaction Steps
Starting from 4.53 g (14.6 mmol) of lithium (1Z)-4-ethoxy-3,4-dioxo-1-[3-(trifluoro-methoxy)phenyl]but-1-en-1-olate from example 3A and 3.56 g (19.8 mmol) of 3-chloro-phenylhydrazine hydrochloride, 1.98 g (4.8 mmol, 33% yield of theory) of product are obtained according to the method described in example 4A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314089B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-dcd8c8e3dc434cd89a0730c26081502e |
| Source note | uspto-grants-2012_11 |