HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylphenylhydrazine monohydrochloride → HCID 58345429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylphenylhydrazine monohydrochloride | HCID 12504 | — |
| Reactant | HCID 58277291 | HCID 58277291 | — |
| Product | HCID 58345429 | HCID 58345429 | 67% |
Reaction Steps
Starting from 631.5 mg (2.15 mmol) of lithium (1Z)-4-ethoxy-3,4-dioxo-1-[3-(trifluoromethyl)phenyl]but-1-en-1-olate from example 1A and 463.2 mg (2.92 mmol) of 4-tolylhydrazine hydrochloride, 535.8 mg (1.4 mmol, 67% yield of theory) of product are obtained according the method described in example 4A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314089B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-16f0358e196c4f8288c6f1a9e9b1961f |
| Source note | uspto-grants-2012_11 |